Charge‐Transport Properties of F6TNAP‐Based Charge‐Transfer Cocrystals

Abstract

The crystal structures of the charge‐transfer (CT) cocrystals formed by the π‐electron acceptor 1,3,4,5,7,8‐hexafluoro‐11,11,12,12‐tetracyanonaphtho‐2,6‐quinodimethane (F6TNAP) with the planar π‐electron‐donor molecules triphenylene (TP), benzo[b]benzo[4,5]thieno[2,3‐d]thiophene (BTBT), benzo[1,2‐b:4,5‐b′]dithiophene (BDT), pyrene (PY), anthracene (ANT), and carbazole (CBZ) have been determined using single‐crystal X‐ray diffraction (SCXRD), along with those of two polymorphs of F6TNAP. All six cocrystals exhibit 1:1 donor/acceptor stoichiometry and adopt mixed‐stacking motifs. Cocrystals based on BTBT and CBZ π‐electron donor molecules exhibit brickwork packing, while the other four CT cocrystals show herringbone‐type crystal packing. Infrared spectroscopy, molecular geometries determined by SCXRD, and electronic structure calculations indicate that the extent of ground‐state CT in each cocrystal is small. Density functional theory calculations predict large conduction bandwidths and, consequently, low effective masses for electrons for all six CT cocrystals, while the TP‐, BDT‐, and PY‐based cocrystals are also predicted to have large valence bandwidths and low effective masses for holes. Charge‐carrier mobility values are obtained from space‐charge limited current (SCLC) measurements and field‐effect transistor measurements, with values exceeding 1 cm2 V−1 s1 being estimated from SCLC measurements for BTBT:F6TNAP and CBZ:F6TNAP cocrystals.

Document Details

Document Type
Pub Defense Publication
Publication Date
Oct 09, 2019
Source ID
10.1002/adfm.201904858

Entities

People

  • Adam J. Matzger
  • Ajith Ashokan
  • Hamna F. Haneef
  • Jean-Luc Brédas
  • Marina S Fonari
  • Oana D. Jurchescu
  • Raghunath Dasari
  • Ren A Wiscons
  • Seth Marder
  • Stephen Barlow
  • Tatiana V Timofeeva
  • Veaceslav Coropceanu
  • Xu Wang
  • Yadong Zhang

Organizations

  • Army Research Office
  • Georgia Tech
  • Institute of Applied Physics
  • National Science Foundation
  • New Mexico Highlands University
  • United States Army Research Laboratory
  • University of Michigan
  • Wake Forest University

Tags

Fields of Study

  • Chemistry
  • Materials science

Readers

  • Materials Science and Engineering.
  • Molecular Photonics/Laser Physics
  • Nanocomposite Materials Science

Technology Areas

  • Microelectronics
  • Space