Catalytic Dealkylation of Ethers to Alcohols on Metal Surfaces

Abstract

On‐surface synthesis has prompted much interest in recent years because it provides an alternative strategy for controlling chemical reactions and allows for the direct observation of reaction pathways. Herein, we combined scanning tunneling microscopy and density functional theory to provide extensive evidence for the conversion of alkoxybenzene‐containing ethers into alcohols by means of surface synthesis. The reported dealkylation reactions are finely controlled by the annealing parameters, which govern the onset of successive alkyl chains dissociations. Moreover, density functional theory calculations elucidate the details of the reaction pathways, showing that dealkylation reactions are surface‐assisted and very different from their homogeneous analogues in solution.

Document Details

Document Type
Pub Defense Publication
Publication Date
Jul 19, 2016
Source ID
10.1002/anie.201602414

Entities

People

  • Biao Yang
  • Haiming Zhang
  • Haiping Lin
  • Jian Fan
  • Kangjian Miao
  • Kewei Sun
  • Liangbo Liang
  • Lifeng Chi
  • Pan Zhu
  • Qing Li
  • Vincent Meunier
  • Youyong Li

Organizations

  • National Natural Science Foundation of China
  • Natural Science Foundation of Jiangsu Province
  • Office of Naval Research
  • Rensselaer Polytechnic Institute

Tags

Readers

  • Combustion science or combustion engineering.
  • Molecular and Cellular Biochemistry
  • Nanoscale Plasmonic Nanotechnology