Maximizing the Catalytic Activity of Nanoparticles through Monolayer Assembly on Nitrogen‐Doped Graphene

Abstract

We report a facile method for assembly of a monolayer array of nitrogen‐doped graphene (NG) and nanoparticles (NPs) and the subsequent transfer of two layers onto a solid substrate (S). Using 3 nm NiPd NPs as an example, we demonstrate that NiPd‐NG‐Si (Si=silicon wafer) can function as a catalyst and show maximum NiPd catalysis for the hydrolysis of ammonia borane (H3NBH3, AB) with a turnover frequency (TOF) of 4896.8 h−1 and an activation energy (Ea) of 18.8 kJ mol−1. The NiPd‐NG‐S catalyst is also highly active for catalyzing the transfer hydrogenation from AB to nitro compounds, leading to the green synthesis of quinazolines in water. Our assembly method can be extended to other graphene and NP catalyst materials, providing a new 2D NP catalyst platform for catalyzing multiple reactions in one pot with maximum efficiency.

Document Details

Document Type
Pub Defense Publication
Publication Date
Dec 07, 2017
Source ID
10.1002/anie.201709815

Entities

People

  • Bo Shen
  • Chao Yu
  • Christopher T Seto
  • Junrui Li
  • Michelle Muzzio
  • Qing Li
  • Shouheng Sun
  • Xuefeng Guo
  • Zheng Xi
  • Zhouyang Yin
  • mengqi shen

Organizations

  • Brown University
  • Huazhong University of Science and Technology
  • National Natural Science Foundation of China
  • United States Army Research Laboratory

Tags

Fields of Study

  • Chemistry

Readers

  • Electrochemical Engineering/ Fuel Cell Technologies
  • Nanocomposite Materials Science

Technology Areas

  • Biotechnology
  • Microelectronics
  • Microelectronics - Graphene