Structure Formation and Coupling Reactions of Hexaphenylbenzene and Its Brominated Analog

Abstract

The on‐surface coupling of the prototypical precursor molecule for graphene nanoribbon synthesis, 6,11‐dibromo‐1,2,3,4‐tetraphenyltriphenylene (C42Br2H26, TPTP), and its non‐brominated analog hexaphenylbenzene (C42H30, HPB), was investigated on coinage metal substrates as a function of thermal treatment. For HPB, which forms non‐covalent 2D monolayers at room temperature, a thermally induced transition of the monolayer's structure could be achieved by moderate annealing, which is likely driven by π‐bond formation. It is found that the dibrominated carbon positions of TPTP do not guide the coupling if the growth occurs on a substrate at temperatures that are sufficient to initiate C−H bond activation. Instead, similar one‐dimensional molecular structures are obtained for both types of precursors, HPB and TPTP.

Document Details

Document Type
Pub Defense Publication
Publication Date
Jul 18, 2021
Source ID
10.1002/cphc.202100049

Entities

People

  • Alexander Sinitskii
  • Axel Enders
  • Christoph Dobner
  • Jacob D Teeter
  • Mamun Sarker
  • Paulo S. Costa

Organizations

  • National Science Foundation
  • Office of Naval Research
  • University of Bayreuth
  • University of Nebraska–Lincoln

Tags

Fields of Study

  • Chemistry

Readers

  • Microwave Engineering.
  • Polymer Science and Technology
  • Quantum Chemistry

Technology Areas

  • Microelectronics
  • Microelectronics - Graphene