Synthesis, Characterization and Properties of Ureido‐Furazan Derivatives
Abstract
The reaction of a variety of amino‐furazans with chlorosulfonyl isocyanate was carried out to synthesize ureido‐furazans. The nitration to nitro‐ureido‐furazan was successful in the case of 3‐nitro‐4‐nitroureido‐furazan and 3,4‐dinitroureido‐furazan. Furthermore, furazan derivatives linked to a second amino‐oxadiazole were synthesized. All compounds were intensively characterized by X‐ray diffraction measurements, NMR spectroscopy, vibrational spectroscopy (IR, Raman), BAM sensitivity tests and differential thermal analysis. The energetic properties were calculated using Explo5 6.03.
Document Details
- Document Type
- Pub Defense Publication
- Publication Date
- Feb 17, 2018
- Source ID
- 10.1002/jhet.3109
Entities
People
- Burkhard Krumm
- Jörg Stierstorfer
- Thomas M. Klapötke
- Tobias S. Hermann
Organizations
- Ludwig-Maximilians-Universität München
- Office of Naval Research