Co-introduction of precipitate hardening and TRIP in a TWIP high-entropy alloy using friction stir alloying
Abstract
Tuning deformation mechanisms is imperative to overcome the well-known strength-ductility paradigm. Twinning-induced plasticity (TWIP), transformation-induced plasticity (TRIP) and precipitate hardening have been investigated separately and have been altered to achieve exceptional strength or ductility in several alloy systems. In this study, we use a novel solid-state alloying method—friction stir alloying (FSA)—to tune the microstructure, and a composition of a TWIP high-entropy alloy by adding Ti, and thus activating site-specific deformation mechanisms that occur concomitantly in a single alloy. During the FSA process, grains of the as-cast face-centered cubic matrix were refined by high-temperature severe plastic deformation and, subsequently, a new alloy composition was obtained by dissolving Ti into the matrix. After annealing the FSA specimen at 900 °C, hard Ni–Ti rich precipitates formed to strengthen the alloy. An additional result was a Ni-depleted region in the vicinity of newly-formed precipitates. The reduction in Ni locally reduced the stacking fault energy, thus inducing TRIP-based deformation while the remaining matrix still deformed as a result of TWIP. Our current approach presents a novel microstructural architecture to design alloys, an approach that combines and optimizes local compositions such that multiple deformation mechanisms can be activated to enhance engineering properties.
Document Details
- Document Type
- Pub Defense Publication
- Publication Date
- Jan 15, 2021
- Source ID
- 10.1038/s41598-021-81350-0
Entities
People
- Bharat Gwalani
- Michael J. Frank
- Rajiv S. Mishra
- Saket Thapliyal
- Shivakant Shukla
- Subhasis Sinha
- Tianhao Wang
Organizations
- National Science Foundation
- United States Army Research Laboratory