Time resolved in-situ multi-contrast X-ray imaging of melting in metals

Abstract

In this work, the application of a time resolved multi-contrast beam tracking technique to the investigation of the melting and solidification process in metals is presented. The use of such a technique allows retrieval of three contrast channels, transmission, refraction and dark-field, with millisecond time resolution. We investigated different melting conditions to characterize, at a proof-of-concept level, the features visible in each of the contrast channels. We found that the phase contrast channel provides a superior visibility of the density variations, allowing the liquid metal pool to be clearly distinguished. Refraction and dark-field were found to highlight surface roughness formed during solidification. This work demonstrates that the availability of the additional contrast channels provided by multi-contrast X-ray imaging delivers additional information, also when imaging high atomic number specimens with a significant absorption.

Document Details

Document Type
Pub Defense Publication
Publication Date
Jul 15, 2022
Source ID
10.1038/s41598-022-15501-2

Entities

People

  • Adam Doherty
  • Alessandro Olivo
  • Christoph Rau
  • Joachim Schulz
  • Lorenzo Massimi
  • Marco Endrizzi
  • Peter D. Lee
  • Samuel J. Clark
  • Saurabh M. Shah
  • Sebastian Marussi
  • Shashidhara Marathe

Organizations

  • Engineering and Physical Sciences Research Council
  • European Commission
  • Royal Academy of Engineering

Tags

Fields of Study

  • Physics

Readers

  • Human-Computer Interaction (HCI).
  • Nanoscale Plasmonic Nanotechnology
  • Surface Engineering/Surface Coating Technology.