Unzipped graphene nanoribbons as sensitive O2 sensors: Electron spin resonance probing and dissociation kinetics

Abstract

Electron spin resonance study of unzipped graphene nanoribbons (GNRs) reveals a specific carbon-related signal, denoted GC, at g=2.0032, attributed to GNRs periphery centers. The signal is observed to be readily quenched upon O2 adsorption, which appears to be fully reversible upon room temperature vacuum treatment. Its depassivation behavior, observed from 130 K onward, is well described by first-order kinetics, characterized by the dissociation energy of 0.58±0.04 eV of spread 0.11±0.02 eV. The GC signal is not sensitive to other gases, such as H2, He, N2, and Ar, pointing to a GC–O2 physisorption interaction unique for GNRs, in agreement with theoretical insight. The GC center thus emerges as a highly selective, sensitive, and reversible O2 sensor.

Document Details

Document Type
Pub Defense Publication
Publication Date
Feb 21, 2011
Source ID
10.1063/1.3559229

Entities

People

  • A. Stesmans
  • Andrew Higginbotham
  • D. V. Kosynkin
  • J. M. Tour
  • K. Keunen
  • Sohail Rao

Organizations

  • Katholieke Universiteit Leuven
  • Office of Naval Research
  • Rice University

Tags

Fields of Study

  • Physics

Readers

  • Aerospace Research.
  • Molecular Photonics/Laser Physics
  • Quantum spin resonance or Electron Paramagnetic Resonance spectroscopy.

Technology Areas

  • Microelectronics