Direct observation of basal-plane to threading-edge dislocation conversion in 4H-SiC epitaxy

Abstract

The propagation behavior of basal plane dislocations from off-oriented 4H-SiC substrates into homoepitaxial layers has been investigated using transmission electron microscopy (TEM), secondary electron microscopy (SEM), and chemical etching. Cross-sectional TEM shows that basal plane dislocations in the substrate are dissociated into pairs of partial dislocations separated by a stacking fault with a width of about 40 nm. Near the substrate/epilayer interface, where most of the basal plane dislocations convert to threading edge dislocations, the two partials constrict before converting. Threading edge segments are inclined by about 20° from the c-axis toward the down-step direction. It is concluded that the critical and limiting step of the dislocation conversion process is constriction of the dissociated partials. Growth surface morphology at the emergence point of the basal plane dislocation was imaged using SEM and is thought to play an important role in the constriction.

Document Details

Document Type
Pub Defense Publication
Publication Date
May 01, 2011
Source ID
10.1063/1.3579447

Entities

People

  • Charles. R. Eddy Jr.
  • D. Kurt Gaskill
  • Marek Skowronski
  • Ping Wu
  • Rachael Myers-ward
  • Suk Chung
  • Virginia D. Wheeler
  • Yoosuf N. Picard

Organizations

  • Carnegie Mellon University
  • II-VI Incorporated
  • Office of Naval Research
  • United States Naval Research Laboratory

Tags

Fields of Study

  • Materials science

Readers

  • Materials Science and Engineering.
  • Semiconductor Device Technology

Technology Areas

  • Microelectronics