Effect of microstructure on irradiated ferroelectric thin films

Abstract

This work investigates the role of microstructure on radiation-induced changes to the functional response of ferroelectric thin films. Chemical solution-deposited lead zirconate titanate thin films with columnar and equiaxed grain morphologies are exposed to a range of gamma radiation doses up to 10 Mrad and the resulting trends in functional response degradation are quantified using a previously developed phenomenological model. The observed trends of global degradation as well as local rates of defect saturation suggest strong coupling between ferroelectric thin film microstructure and material radiation hardness. Radiation-induced degradation of domain wall motion is thought to be the major contributor to the reduction in ferroelectric response. Lower rates of defect saturation are noted in samples with columnar grains, due to increased grain boundary density offering more sites to act as defect sinks, thus reducing the interaction of defects with functional material volume within the grain interior. Response trends for measurements at low electric field show substantial degradation of polarization and piezoelectric properties (up to 80% reduction in remanent piezoelectric response), while such effects are largely diminished at increased electric fields, indicating that the defects created/activated are primarily of low pinning energy. The correlation of film microstructure to radiation-induced changes to the functional response of ferroelectric thin films can be leveraged to tune and tailor the eventual properties of devices relying on these materials.

Document Details

Document Type
Pub Defense Publication
Publication Date
Jun 23, 2017
Source ID
10.1063/1.4987032

Entities

People

  • Cory D. Cress
  • Elizabeth A. Paisley
  • Evan R. Glaser
  • Hanhan Zhou
  • Jacob L. Jones
  • Jon F. Ihlefeld
  • Manuel Rivas
  • Nazanin Bassiri-Gharb
  • Ronald G. Polcawich
  • Ryan Q. Rudy
  • Samuel C Williams
  • Steven J. Brewer

Organizations

  • Defense Threat Reduction Agency
  • Georgia Tech
  • North Carolina State University
  • Sandia National Laboratories
  • United States Army Research Laboratory
  • United States Naval Research Laboratory

Tags

Fields of Study

  • Physics

Readers

  • Materials Science and Engineering.
  • Nuclear and Radiation Engineering.
  • Structural Health Monitoring of Composite Structures.