Communication: Water activation and splitting by single metal-atom anions

Abstract

We report experimental and computational results pertaining to the activation and splitting of single water molecules by single atomic platinum anions. The anion photoelectron spectra of [Pt(H2O)]−, formed under different conditions, exhibit spectral features that are due to the anion-molecule complex, Pt−(H2O), and to the reaction intermediates, HPtOH− and H2PtO−, in which one and two O–H bonds have been broken, respectively. Additionally, the observations of PtO− and H2+ in mass spectra strongly imply that water splitting via the reaction Pt− + H2O → PtO− + H2 has occurred. Extending these studies to nickel and palladium shows that they too are able to activate single water molecules, as evidenced by the formation of the reaction intermediates, HNiOH− and HPdOH−. Computations at the coupled cluster singles and doubles with perturbatively connected triples level of theory provide structures and vertical detachment energies (VDEs) for both HMOH− and H2MO− intermediates. The calculated and measured VDE values are in good agreement and thus support their identification.

Document Details

Document Type
Pub Defense Publication
Publication Date
Dec 10, 2018
Source ID
10.1063/1.5050913

Entities

People

  • Evangelos Miliordos
  • Gaoxiang Liu
  • Kit H Bowen
  • Martin Tschurl
  • Sandra M Ciborowski
  • Sotiris Xantheas
  • Ulrich Boesl
  • Ulrich Heiz
  • Xinxing Zhang

Organizations

  • Air Force Office of Scientific Research
  • Division of Chemistry
  • Johns Hopkins University
  • Nankai University
  • Pacific Northwest National Laboratory
  • Technical University of Munich
  • United States Department of Energy
  • University of Washington

Tags

Fields of Study

  • Chemistry

Readers

  • Electrochemical Engineering/ Fuel Cell Technologies
  • Molecular Photonics/Laser Physics
  • Quantum spin resonance or Electron Paramagnetic Resonance spectroscopy.

Technology Areas

  • Microelectronics