Novel spatially coordinated in-situ Raman and nanoscale wear analysis of FCVA-deposited DLC film

Abstract

A novel combined in-situ system, integrating Raman spectroscopy and depth-sensing techniques, was applied to analyze the wear induced transformation on the microstructure of diamond-like carbon (DLC) film deposited on Si substrates using a filtered cathodic arc vacuum (FCVA) deposition system. Using this synchronized characterization technique it was demonstrated that upon wear-induced removal of upper surface layers, the intensity ratio (ID/IG) for the area inside wear tracks decreases. On the other hand, while the peak position for the D line (PD) shifts to higher wavenumbers, the peak position for the G line (PG) shifts to lower wavenumbers. The coefficient of friction shows significant reduction upon increasing the depth of the wear tracks. These results confirm our previous preliminary report on the possible existence of layers rich in sp2 in the surface region. It was also shown that the wear debris is more graphitized.

Document Details

Document Type
Pub Defense Publication
Publication Date
Jun 01, 2019
Source ID
10.1063/1.5107474

Entities

People

  • Franklin Chau-nan Hong
  • Jonathan Hobley
  • M. Djafari Rouhani
  • Yeau-Ren Jeng

Organizations

  • Air Force Office of Scientific Research
  • National Cheng Kung University
  • National Chung Cheng University
  • National Science and Technology Council

Tags

Fields of Study

  • Materials science

Readers

  • Materials Science and Engineering.
  • Nanoscale Plasmonic Nanotechnology
  • Tribology (the study of the boundary interaction between sliding surfaces, lubrication, wear and friction).