Mediation of donor–acceptor distance in an enzymatic methyl transfer reaction

Abstract

During the past 30 years, the methyl transfer community has attempted to find the molecular origin of the methyltransferases’ catalytic power. This report describes a combination of experimental and computational studies of enzymatic methyl transfer catalyzed by catechol- O -methyltransferase and its mutants at position Tyr68. The results show structural and dynamical differences between WT and mutants, as well as a role for substrate ionization in the generation of active site compaction. For the first time, to our knowledge, we are able to show a trend in donor–acceptor distance in the ground state that can be correlated with catalytic efficiency. This work provides an important step forward and a clear new direction for understanding enzymatic methyl transfer.

Document Details

Document Type
Pub Defense Publication
Publication Date
Jun 15, 2015
Source ID
10.1073/pnas.1506792112

Entities

People

  • Heather J. Kulik
  • Jianyu Zhang
  • Judith P. Klinman
  • Todd Martinez

Organizations

  • Burroughs Wellcome Fund
  • California Institute for Quantitative Biosciences
  • National Institutes of Health
  • Stanford University
  • United States Department of Defense
  • Yusuf Hamied Department of Chemistry

Tags

Readers

  • Molecular and Cellular Biochemistry
  • Molecular and genetic basis of cancer.
  • Theoretical Analysis.