Crystal structure engineering in multimetallic high-index facet nanocatalysts

Abstract

Crystal structure engineering in nanoparticles represents an important strategy in catalyst design, as catalytic performance is highly dependent on atomic arrangement. However, realizing crystal structure engineering in high-index facet nanocatalysts has been a synthetic challenge for decades. Here, we first employed density functional theory calculations to determine whether surface modifications can stabilize high-index facets during crystal structure transformations and then synthesized a library of multimetallic high-index facet tetrahexahedral (THH) nanoparticles with controllable crystal structures. Importantly, the crystal structural transition between the intermetallic and chemically disordered states is reversable, and the THH morphology of nanocatalysts is maintained during this transformation. This approach broadens the synthetic scope of nanocatalysts available for use in diverse chemical processes.

Document Details

Document Type
Pub Defense Publication
Publication Date
Jun 23, 2021
Source ID
10.1073/pnas.2105722118

Entities

People

  • Bo Shen
  • Chad Mirkin
  • Chris Wolverton
  • Cindy Y Zheng
  • Jiahong Shen
  • Kun He
  • Liliang Huang
  • Vinayak P. Dravid

Organizations

  • Air Force Office of Scientific Research
  • National Science Foundation
  • Northwestern University
  • Sherman Fairchild Foundation
  • United States Department of Energy

Tags

Fields of Study

  • Chemistry

Readers

  • Materials Science and Engineering.
  • Nanoscale Plasmonic Nanotechnology
  • Quantum Dot Semiconductor Device Photonics and Graphene Optoelectronic Materials and THz Physics.

Technology Areas

  • Biotechnology