Quantitative detection of hydrogen peroxide in rain, air, exhaled breath, and biological fluids by NMR spectroscopy

Abstract

Hydrogen peroxide (H 2 O 2 ) plays a key role in environmental chemistry, biology, and medicine. H 2 O 2 concentrations typically are 6 to 10 orders of magnitude lower than that of water, making its quantitative detection challenging. We demonstrate that optimized NMR spectroscopy allows direct, interference-free, quantitative measurements of H 2 O 2 down to submicromolar levels in a wide range of fluids, ranging from exhaled breath and air condensate to rain, blood, urine, and saliva. NMR measurements confirm the previously reported spontaneous generation of H 2 O 2 in microdroplets that form when condensing water vapor on a hydrophobic surface, which can interfere with atmospheric H 2 O 2 measurements. Its antimicrobial activity and strong seasonal variation speculatively could be linked to the seasonality of respiratory viral diseases.

Document Details

Document Type
Pub Defense Publication
Publication Date
Feb 14, 2022
Source ID
10.1073/pnas.2121542119

Entities

People

  • Ad Bax
  • Belhu Metaferia
  • Richard Zare
  • Tayeb Kakeshpour

Organizations

  • Air Force Office of Scientific Research
  • National Institute of Diabetes and Digestive and Kidney Diseases
  • Stanford University

Tags

Fields of Study

  • Chemistry
  • Environmental science

Readers

  • Aerosol Science/Aerosol Physics
  • Electrochemical Engineering/ Fuel Cell Technologies
  • Immunology and Pathology