A mail-in and user facility for X-ray absorption near-edge structure: the CEI-XANES laboratory X-ray spectrometer at the University of Washington

Abstract

There are more than 100 beamlines or endstations worldwide that frequently support X-ray absorption fine-structure (XAFS) measurements, thus providing critical enabling capability for research across numerous scientific disciplines. However, the absence of a supporting tier of more readily accessible, lower-performing options has caused systemic inefficiencies, resulting in high oversubscription and the omission of many scientifically and socially valuable XAFS applications that are incompatible with the synchrotron facility access model. To this end, this work describes the design, performance and uses of the Clean Energy Institute X-ray absorption near-edge structure (CEI-XANES) laboratory spectrometer and its use as both a user-present and mail-in facility. Such new additions to the XAFS infrastructure landscape raise important questions about the most productive interactions between synchrotron radiation and laboratory-based capabilities; this can be discussed in the framework of five categories, only one of which is competitive. The categories include independent operation on independent problems, use dictated by convenience, pre-synchrotron preparatory use of laboratory capability, post-synchrotron follow-up use of laboratory capability, and parallel use of both synchrotron radiation and laboratory systems.

Document Details

Document Type
Pub Defense Publication
Publication Date
Oct 23, 2019
Source ID
10.1107/s1600577519012839

Entities

People

  • Alexander S. Ditter
  • Evan P. Jahrman
  • Gerald T. Seidler
  • Liam R. Bradshaw
  • Peter J. Pauzauskie
  • Xiaojing Xia

Organizations

  • Air Force Office of Scientific Research
  • National Science Foundation
  • Office of Science
  • University of Washington

Tags

Fields of Study

  • Physics

Readers

  • Research Science/Academic Research
  • Systems Analysis and Design