9-(3,5-Dimethylbenzylidene)-8-(3,5-dimethylphenyl)-1,3,5,7-tetraphenyl-2,4,7,8-tetrahydro-4,7-methanoazulene acetonitrile disolvate
Abstract
The title Diels–Alder product, C52H44·2CH3CN, was obtained in trace quantity as the `endo' isomer during the synthesis of 1,3-diphenyl-6-(3,5-dimethylphenyl)fulvene. One of the two co-crystallized acetonitrile molecules is linked to the main molecule by a weak C—H...N hydrogen bond.
Document Details
- Document Type
- Pub Defense Publication
- Publication Date
- Apr 17, 2018
- Source ID
- 10.1107/s2414314618005539
Entities
People
- Andrew J Peloquin
- Gary J Balaich
- Scott T Iacono
- Sonya K. Adas
Organizations
- Air Force Office of Scientific Research
- Defense Threat Reduction Agency