Optical constants of germanium and thermally grown germanium dioxide from 0.5 to 6.6eV via a multisample ellipsometry investigation

Abstract

Thermal GeO2 oxides up to 136 nm thickness were produced by annealing Ge wafers in pure oxygen at 550 °C and 270 kPa pressure for up to 10 h. The oxidation kinetics followed the Deal–Grove law. Using multisample spectroscopic ellipsometry for a series of five thermal oxides with different thicknesses, the complex dielectric functions of Ge and GeO2 were determined from 0.5 to 6.6 eV, for thin-film metrology applications in Ge-based microelectronics and photonics. The dispersion of the GeO2 layer was modeled with a simple Tauc-Lorentz oscillator model, but a more complicated dispersion with eight parametric oscillators was required for Ge. A reasonable fit to the ellipsometric angles could be obtained by assuming that all thermal oxides can be described by the same dielectric function, regardless of thickness, but a slight improvement was achieved by allowing for a lower density oxide near the surface of the thickest films. The authors compare their results with literature data for Ge and bulk and thin-film GeO2.

Document Details

Document Type
Pub Defense Publication
Publication Date
Sep 30, 2016
Source ID
10.1116/1.4963075

Entities

People

  • Amber A. Medina
  • Cayla M. Nelson
  • Jaime M. Moya
  • Nalin S. Fernando
  • Nuwanjula S. Samarasingha
  • Stefan Zollner
  • T. Nathan Nunley

Organizations

  • Air Force Office of Scientific Research
  • Army Research Office
  • National Science Foundation
  • New Mexico State University

Tags

Fields of Study

  • Materials science

Readers

  • Optical Physics and Photonics.
  • Statistical inference.
  • Thin Film Deposition Science.

Technology Areas

  • Microelectronics
  • Microelectronics - Graphene