Communication—Microfluidic Electrochemical Acetylcholine Detection in the Presence of Chlorpyrifos

Abstract

An amperometric acetylcholine sensor was developed for use in a microfluidic system and characterized with chlorpyrifos and its metabolite, chlorpyrifos oxon. This enzymatic sensor was highly selective for acetylcholine, with a detection limit of 0.2 μM and sensitivity of 1.7 nA μM−1from 1–150 μM. Though chlorpyrifos had no effect on sensor function, chlorpyrifos oxon significantly inhibited response across a range of concentrations (0.5–50 μM). Inhibition was reversed by 2-pyridine aldoxime methyl chloride. This platform can be used to both quantify acetylcholine in the presence of chlorpyrifos and as a biorecognition method for chlorpyrifos oxon.

Document Details

Document Type
Pub Defense Publication
Publication Date
Jan 01, 2019
Source ID
10.1149/2.0711916jes

Entities

People

  • David Cliffel
  • Dusty R. Miller
  • Ethan S. McClain

Organizations

  • Intelligence Advanced Research Projects Activity

Tags

Readers

  • Analytical Chemistry
  • Nanoscale Plasmonic Nanotechnology
  • Neurotoxicology