COPPER AS A PHOTOMETRIC INDICATOR IN THE SELECTIVE CHELOMETRIC TITRATION OF METAL ION MIXTURES

Abstract

Photometric and point detection permits selective chelometric determination of metal ions in mixtures with much less masking than required for visual or potentiometric techniques. Copper has been found to be a useful photometric indicator for such titrations. Prediction of appropriate titration conditions is readily accomplished with graphical plots of effective chelonate stability. Calcium is determined in the presence of magnesium with ethylene glycol bis(beta-aminoethyl ether)-N,N-tetraacetic acid in 0.5 M ammonium hydroxide at pH 10. Selective determination of cadmium or of zinc in the presence of the other is carried out with diethylenetriaminepentaacetic acid under the same conditions. Attention is directed to the importance of competitive equilibria which affect chelonate stability, and stability constants for ammonia derivatives of some copper chelonates are reported. (Author)

Document Details

Document Type
Technical Report
Publication Date
Mar 02, 1961
Accession Number
AD0255479

Entities

People

  • David A. Aikens
  • Gaby Schmuckler

Organizations

  • University of North Carolina at Chapel Hill

Tags

DTIC Thesaurus Topics

  • Alkenes
  • Chemical Compounds
  • Detection
  • Ethylene Glycol
  • Ethylenes
  • Glycols
  • Hydroxides
  • Indicators
  • Magnesium
  • Metals
  • Organic Compounds
  • Titration

Fields of Study

  • Chemistry

Readers

  • Analytical Chemistry
  • Surface Engineering/Surface Coating Technology.