STUDY OF THE ADDITION REACTION BETWEEN TRIALKOXYSILANES AND OLEFINS

Abstract

The addition of trialkoxysilanes to olefins was demonstrated by interacting triethoxysilane, triisopropoxysilane, tributoxysilane, tri(sec-butoxy)-silane, and tri(tert-butoxy)silane with 1-nonene and 1-decene in the presence of chloroplatinic acid and platinized charcoal. In the presence of chloroplatinic acid a yield of 30 to 40% was obtained. The addition of tri(tert-butoxy)silane, due to steric hindrance, gave the lowest yields of all (12%). Decyltributoxysilane and nonyltriisopropoxysilane were also obtained by direct synthesis, by the reaction of nonyltrichlorosilane and decyltrichlorosilane with the corresponding alcohols. The physicochemical properties of the alkyl-trialkoxysilanes obtained by both methods, addition to olefins and reaction with alcohols, were identical.

Document Details

Document Type
Technical Report
Publication Date
Oct 01, 1960
Accession Number
AD0257140

Entities

People

  • A.v. Topchiyev
  • N.s. Nametkin

Organizations

  • National Air and Space Intelligence Center

Tags

DTIC Thesaurus Topics

  • Addition Reactions

Fields of Study

  • Chemistry

Readers

  • Chemistry (specifically Chemical Fluorescence)
  • Organic Chemistry