MECHANISM OF ENZYME ACTION

Abstract

THE SUCCESSFUL SYNTHESIS OF 5(OR 6)-VINYL BENZIMIDAZOLE IS DESCRIBED. This monomer was prepared via a route which started with beta(4-formanilino)-ethyl formate. The final step was dehydrochlorination of 5(or 6)-(betachloroethyl)-benzimidazole. Structure of the monomer was proven by elemental analysis, derivatives, hydrogenation and ozonolysis. Attempts to prepare copolymers of 4-vinyl imidazole and allyl alcohol by reduction of the methyl acrylate copolymers are described. Also reported are attempts to prepare 1-methyl-4 (or 5)-vinyl imidazole and copolymers of 4-vinyl imidazole and vinylene carbonate. The successful synthesis of copolymers with acrylic acid and of poly(4-vinyl imidazole) are reported. Some kinetic studies of the hydrolysis of p-nitrophenyl acetate catalyzed by imidazolecontaining polymers are reported. All polymers tested were slower than imidazole itself. It is concluded that no enhancement of catalytic activity was found in the few polymers tested. The synthesis of new polymers is in progress. (Author)

Document Details

Document Type
Technical Report
Publication Date
Jun 30, 1961
Accession Number
AD0264911

Entities

People

  • Bernhard Kosters
  • C.g. Overberger
  • Norman Vorchheimer

Organizations

  • New York University Tandon School of Engineering

Tags

DTIC Thesaurus Topics

  • Acids
  • Acrylates
  • Acrylic Acid
  • Alkenes
  • Benzimidazoles
  • Carbonates
  • Chemical Compounds
  • Copolymers
  • Hydrogenation
  • Hydrolysis
  • Imidazoles
  • Organic Compounds
  • Polymers

Fields of Study

  • Chemistry

Readers

  • Electrochemical Engineering/ Fuel Cell Technologies
  • Neurotoxicology
  • Polymer Science and Technology

Technology Areas

  • Microelectronics