THE THERMAL DECOMPOSITION OF PERCHLORIC ACID VAPOR

Abstract

The thermal decomposition of perchloric acid vapor has been studied from 200 to 439 C. The reaction products over this temperature range have been found to be chlorine, water and oxygen. From 200 to 350 C the kinetics of the decomposition reaction have been studied by determining the rate of chlorine formation colorimetrically; from 350 to 439 C the kinetics were determined by a flow system technique. The results of the kinetic measurements are interpreted in terms of a heterogeneous reaction at the lower temperatures and a homogeneous one at the higher temperatures. A mechanism for the homogeneous reaction is proposed. (Author)

Document Details

Document Type
Technical Report
Publication Date
Oct 04, 1961
Accession Number
AD0265051

Entities

People

  • Joseph B. Levy

Organizations

  • ARCO

Tags

DTIC Thesaurus Topics

  • Acids
  • Chlorine
  • Decomposition
  • Kinetics
  • Measurement
  • Perchloric Acid

Readers

  • Analytical Chemistry
  • Combustion science or combustion engineering.