REDUCTION AND CONSOLIDATION OF SUPERIOR QUALITY MOLYBDENUM ALLOYS

Abstract

The problem encountered in electron-beam melting of molybdenum, particularly that containing calcium and calcium oxide, has been largely overcome by improvements made both in the starting material and in the design of the electron-beam furnace and gun. Starting material was vacuum sintered to remove a large portion of the volatile material. The use of a remote gun, accelerating anode, and focusing coils permitted melting of the sintered material at reasonable rates. Molybdenum sheet rolled from a single crystal was found to have a recrystallization temperature between 1400 and 1600 F. The asrolled sheet exhibited low room temperature ductility. However, following a one hour anneal at 1400 F, the ductility was significantly improved. Molybdenum sheet was produced by powder metallurgy techniques using inert handling and vacuum sintering. Considerable ductility was obtained in the longitudinal and transverse directions from 0.048-in. sheet. Recrystallization temperature of this material is approximately 2200 F. (Author)

Document Details

Document Type
Technical Report
Publication Date
Apr 30, 1961
Accession Number
AD0265364

Entities

People

  • D.s. Fairgrieve
  • Edmund Baroch
  • James Wong

Organizations

  • Bell Aircraft Corporation

Tags

DTIC Thesaurus Topics

  • Advanced Materials
  • Biomedical And Dental Materials
  • Crystals
  • Ductility
  • Electron Beam Melting
  • Electron Beams
  • Electrons
  • Fabrication
  • Manufacturing
  • Materials
  • Materials Processing
  • Materials Science
  • Molybdenum
  • Molybdenum Alloys
  • Powder Metallurgy
  • Single Crystals
  • Transition Temperature

Fields of Study

  • Materials science

Readers

  • Materials Science and Engineering.
  • Superconducting Magnet Technology
  • Thin Film Deposition Science.

Technology Areas

  • Directed Energy
  • Microelectronics
  • Microelectronics - Graphene