ELECTRON AND LIGHT MICROSCOPY TECHNIQUES SUITABLE FOR STUDYING FATIGUE DAMAGE IN A CRYSTALLIZED GLASS CERAMIC

Abstract

Identifiers: Pyroceram. New techniques and methods making it possible to study the rolling-fatigue process in Pyroceram were developed. A method for locating, orienting, and identifying specific areas to be viewed by the electron microscope is outlined. A replication technique is described which makes use of preshadowed silicon monoxide replicas deposited after the application of a releasing agent. A vibratory polishing technique was found to produce surfaces free of all evidences of fire-polishing, even when examined by electron microscopy. A satisfactory stain was found that reduces the glare of reflected light when examining Pyroceram specimens with the light microscope. (Author)

Document Details

Document Type
Technical Report
Publication Date
Nov 01, 1961
Accession Number
AD0266703

Entities

People

  • Erwin V. Zaretsky
  • Shelley Harrell

Organizations

  • National Aeronautics and Space Administration

Tags

Communities of Interest

  • Materials and Manufacturing Processes

DTIC Thesaurus Topics

  • Electron Microscopes
  • Electron Microscopy
  • Electrons
  • Microscopes
  • Microscopy
  • Monoxides
  • Polishing
  • Replicas

Readers

  • Powder metallurgy of Titanium alloys.
  • Surface Coatings Technology.
  • Vision Science/Vision Psychology/Cognitive Neuroscience.

Technology Areas

  • Microelectronics
  • Microelectronics - Graphene