SUBSTRUCTURE AND MECHANICAL PROPERTIES OF REFRACTORY METALS

Abstract

Quantitative results on the substructural characteristics of W, Mo, Ta and Co are being obtained through the coordinated programs of the five laboratories. Changes in subboundary spacing of worked materials were measured microscopically as a function of annealing temperature, and corresponding changes in particle size and lattice strain were obtained by Fourier analyses of diffraction-line shapes. Combined application of x-ray reflection microscopy, double-crystal diffractometry, and transmission electron microscopy to single-crystal and polycrystalline W revealed various orders of substructure in terms of size, disorientation, and dislocation arrays; and progressive alterations were traced through the stages of recovery and recrystallization. Stacking faults and twins have been found in W and Co after high-temperature annealing. The complex interfolding of the distorted grains and the formation of deformation bands produce an unexpectedly large number of boundary intercepts per unit of transverse distance. (Author)

Document Details

Document Type
Technical Report
Publication Date
Aug 01, 1961
Accession Number
AD0266881

Entities

People

  • B.s. Lement
  • D.a. Thomas

Tags

DTIC Thesaurus Topics

  • Annealing
  • Crystals
  • Electron Microscopy
  • Fourier Analysis
  • High Temperature
  • Materials
  • Mechanical Properties
  • Microscopy
  • Particle Size
  • Particles
  • Refractory Metals
  • Single Crystals
  • Transition Temperature
  • Transmission Electron Microscopy
  • X Rays

Fields of Study

  • Materials science
  • Physics

Readers

  • Materials Science and Engineering.

Technology Areas

  • Microelectronics
  • Space