THE IDENTIFICATION OF SOME PRODUCTS PRODUCED ON STORING TRICHLOROETHYLENE

Abstract

Trichloroethylene, stored for an extended period in contact with aqueous NaOH, was found to acidify pure water. Experiments were carried out to determine whether this effect was due to spontaneous hydrolysis or to extraction of acids produced during storage. Samples of stored trichloroethylene and of freshly purified trichloroethylene were stirred with conductivity water, and pH was measured as a function of time. Freshly purified trichloroethylene did not decrease the pH of the water. The rate and degree of extraction of acids from the stored trichloroethylene varied with the initial pH. Hydrochloric and glyoxylic acids were identified among the acids produced during extended storage of trichloroethylene with base. (Author)

Document Details

Document Type
Technical Report
Publication Date
Aug 01, 1961
Accession Number
AD0268885

Entities

People

  • James Harris
  • Nathan Klein
  • Ronald A. Sasse'

Tags

DTIC Thesaurus Topics

  • Alkenes
  • Chemical Compounds
  • Conductivity
  • Extraction
  • Glyoxylic Acid
  • Hydrolysis
  • Identification
  • Organic Compounds

Readers

  • Analytical Chemistry