RESEARCH STUDY TO DETERMINE THE PHASE EQUILIBRIUM RELATIONS OF SELECTED METAL CARBIDES AT HIGH TEMPERATURES

Abstract

INVESTIGATIONS WERE MADE OF PHASE EQUILIBRIA IN THE BINARY SYSTEMS, W-C and Zr-C. A completed phase diagram for the W-C system is presented which differs significantly from the one proposed by Sykes (Trans. Am. Soc. Steel Treating 18:968, 1930) and which is generally accepted today. A tentative phase diagram for the Zr-C system i included. Data were obtained by hightemperature differential thermal analysis and classical quenching procedures, both supplemented by metallographic, X-ray, and chemical techniques. Resulbetween W and W2C at 2710 C and between W2C and beta-WC at 2765 C. The W2C lattice accommodates 7 and 74 at-% W at 2460 nd 2710 C, respectively. Carbon solubility is evident only a 2525 C, the eutectoid temperature. The melting point of W2C was found to be 2795 C. At 2755 C, WC decomposes into beta-WC and graphite. A new cubic phase (beta-WC) has been discovered which is stable only above 2525 s for the W-C binary system indicate eutectics between W and W2C at 2710 C and between W2C and beta-WC at 2765 C. The W2C lattice accommodates 7 and 74 at-% W at 2460 nd 2710 C, respectively. Carbon solubility is evident only a 2525 C, the eutectoid temperature. The melting point of W2C was found to be 2795 C. At 2755 C, WC decomposes into beta-WC and graphite. A new cubic phase (beta-WC) has been discovered which is stable only above 2525 C. The Zr-C system is characterized by eutectic temperatures of 1860 and 2850 C on the Zr-rich and C-rich sides of ZrC, respectively. ZrC is the only carbide phase which has been observed in this syst m. (Author)

Document Details

Document Type
Technical Report
Publication Date
Apr 01, 1962
Accession Number
AD0277794

Entities

People

  • R.t. Dolloff
  • R.v. Sara

Tags

DTIC Thesaurus Topics

  • Diagrams
  • Differential Thermal Analysis
  • Graphitic Materials
  • High Temperature
  • Melting
  • Melting Point
  • Phase
  • Phase Diagrams
  • Solubility
  • Thermal Analysis
  • Thermodynamic Processes
  • X Rays

Fields of Study

  • Materials science

Readers

  • Materials Science and Engineering.
  • Surface Engineering/Surface Coating Technology.