LOW TEMPERATURE TENSILE PROPERTIES OF ZONE-REFINED NIOBIUM (COLUMBIUM)

Abstract

Specimens of electron beam zone-refined Nb were subjected to tensile tests in the temperature range from 373 to 4.2 K. Both polycrystalline and single crystalline specimens were tested. Specimens were either deformed to fracture or the temperature was changed during deformation to measure the reversible flow stress. The quantity of impurities remaining in the zone-refined material was ascertained by chemical analyses and the results were checked by resistivity measurements. A significant amount of zone-refining took place even at the relatively high rates of zone travel used (2mm/min.). Twinning was observed in all specimens tested t 4.2 K. No discontinuous yield points were observed in these tests indicating that this phenomenon is dependent upon impurity content. An increased impurity level resulted in a lowering of the yield and flow stresses without an appreciable change in the temperature dependence. This indicates that a lattice frictional stress is the possible mechanism responsible for the temperature dependence of the yield and flow stresses. (Author)

Document Details

Document Type
Technical Report
Publication Date
Jan 01, 1962
Accession Number
AD0278051

Entities

People

  • J.f. Wellings
  • R. Maddin

Organizations

  • University of Pennsylvania

Tags

DTIC Thesaurus Topics

  • Chemical Analysis
  • Electron Beams
  • Electrons
  • Impurities
  • Low Temperature
  • Materials
  • Measurement
  • Niobium
  • Polycrystals
  • Refining
  • Reversible
  • Tensile Properties
  • Yield Strength

Fields of Study

  • Materials science

Readers

  • Materials Science and Engineering.
  • Mechanical Engineering/Mechanics of Materials.

Technology Areas

  • Directed Energy
  • Directed Energy - Pulsed-Laser Deposition
  • Microelectronics