METHODS OF MICROANALYSIS V. OXYGEN FLASK COMBUSTION OF CHEMICAL AGENTS

Abstract

The oxygen flask technique of sample combustion was applied to products produced in Chemical Corps research. Evaluation was obtained through selected and modified microvolumetric procedures. Results were obtained for sulfur and halogen elements. The ranges of analytical recovery for each individual element or procedure were 100% ! 0.29% for the average recovery; less than or equal to 0.35 for the average deviation; less than or equal to 0.28 for the standard deviation.A favorable comparison was found by contrasting these quantities with similar ones obtained by other methods. Optimum design parameters for the flask are considered. (Author)

Document Details

Document Type
Technical Report
Publication Date
Apr 01, 1962
Accession Number
AD0278160

Entities

People

  • John M. Corliss

Organizations

  • Edgewood Chemical Biological Center

Tags

DTIC Thesaurus Topics

  • Chemical Warfare Agents
  • Chemical Weapons
  • Combustion
  • Data Science
  • Information Science
  • Microanalysis
  • Recovery
  • Standards
  • Test And Evaluation

Readers

  • Analytical Chemistry
  • Mathematics or Statistics