SYNTHESIS OF ORGANOSILICON MONOMERS WITH NITRILE GROUPS
Abstract
For the purpose of obtaining new organosilicon monomers with nitrile groups, the addition of Cl3SiH to cyclohexene-3-carbonitrile was studied. The best results in the addition of trichlorosilane to cyclohexenecarbonitrile were obtained when tertiary butyl peroxide was used as a catalyst. The use of IR spectra for the identification of the addition products did not give positive results. Considerable amounts (up to 60-90%) of SiCl4 formed attests to the disproportionation of HSiCl3 under the action of nitrogen-containing compounds present in the reaction mixture. (Author)
Document Details
- Document Type
- Technical Report
- Publication Date
- Oct 26, 1962
- Accession Number
- AD0292663
Entities
People
- A.d. Petrov
- Ye. P. Zakharov
Organizations
- National Air and Space Intelligence Center