Scale-up N2F4-Olefin Reactions in a high pressure liquid phase flow reactor
Abstract
Difluoramino compounds were continuously synthesized by the high pressure liquid phase reaction of N2F4 with an olefin diluted in an appropriate solvent. About 400 pounds of two N2F4 adducts were synthesized over a two-year period in a tubular reactor operating in the laminar flow regime. The productivity of the reactor was progressively increased to a rate of about 100 pounds per month. A mathematical model of the flow reactor was developed and used to establish reaction conditions that would not result in prohibitive exotherms.
Document Details
- Document Type
- Technical Report
- Publication Date
- Dec 03, 1965
- Accession Number
- AD0367626
Entities
People
- Thomas J. Dwyer