A STUDY OF THE ADSORPTION MECHANISMS ON OXYGEN ELECTRODES

Abstract

An improved method for studying the exchange of oxygen with O18 pre- adsorbed on a metal surface is reported. Detailed information on the nature of the chemisorbed oxygen on silver and the isotopic exchange mechanism at 200 C was obtained. The rates of chemisorption and dissociation were determined, which are two distinct processes beyond a certain oxygen coverage. Oxygen pressure versus temperature characteristics and isotopic exchange reactions on carefully cleaned silver and silver-gold alloy powder surfaces are reported. The powders were all prepared by a spark erosion method. A strong increase in the exchange activity was obtained at elevated temperatures by dilution of the silver. With pure silver at room temperature a dissociative oxygen exchange was observed which decreased with time. A palladium powder (of commercial origin) was active only above 100 C.

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Document Details

Document Type
Technical Report
Publication Date
Jan 29, 1963
Accession Number
AD0404296

Entities

People

  • Y. L. Sandler

Tags

Communities of Interest

  • Advanced Electronics
  • Ground and Sea Platforms

DTIC Thesaurus Topics

  • Adsorption
  • Air Force
  • Chemical Synthesis
  • Chemistry
  • Desorption
  • Electronics
  • Electronics Laboratories
  • Exchange Reactions
  • Gold Alloys
  • Low Temperature
  • Materials
  • Measurement
  • Military Research
  • New Jersey
  • New York
  • Oxygen Electrodes
  • Water Vapor

Fields of Study

  • Materials science

Readers

  • Electrochemical Engineering/ Fuel Cell Technologies
  • Plasma Physics.