THE PREPARATION OF HIGH PURITY RARE EARTH METALS BY ZONE REFINING

Abstract

Ultra high purity rare earth metals, Samarium, Europium, Gadolinium with total impurities of less than .1 ppm were attempted. Methods of separation, reduction and purification were: ion exchange, dry fluoride preparation, metallo thermiction, vacuum distillation, zone refining by induction heat and electron beam melting. Gas chromatography was investigated as an analytical tool for determination of oxygen in metals.

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Document Details

Document Type
Technical Report
Publication Date
Jan 31, 1963
Accession Number
AD0405751

Entities

People

  • C. J. Heinink

Tags

Communities of Interest

  • Space

DTIC Thesaurus Topics

  • Air Force
  • Coefficients
  • Detection
  • Distillation
  • Electron Beams
  • Electrons
  • Elements
  • Europium
  • Heat Energy
  • Impurities
  • Ion Exchange
  • Materials
  • Materials Processing
  • Melting
  • Rare Earth Elements
  • Samarium
  • Vapor Pressure

Readers

  • Materials Science and Engineering.
  • Thin Film Deposition Science.

Technology Areas

  • Directed Energy
  • Microelectronics
  • Microelectronics - Graphene