PROSPECTIVE ANTIRADIATION AGENTS
Abstract
The extension of the five-step synthesis of 3-amino-2-methyl-2- butanethiol hydrochloride was described. An investigation of possible reaction of acetylene with 1-carbethoxy-3-pyrrolidone was pursued with the hope of forming an intermediate acetylenic carbinol which would ultimately lead to an aminothiol wherein the amino group would be part of the heterocyclic five- membered ring. The possibilities of forming aminothiols from aminoalkenes formed from Schiff bases was also investigated, but unfortunately, these intermediates failed to react with thiols to produce the described sulfide. The synthesis of aminoalkane thiols was also described.
Document Details
- Document Type
- Technical Report
- Publication Date
- Mar 31, 1963
- Accession Number
- AD0407579
Entities
People
- Gardner W. Stacy
Organizations
- Washington State University