SYNTHESIS OF SELECTED ETHERS, PHENOLS AND RELATED COMPOUNDS HAVING NITROGEN-CONTAINING GROUPS.
Abstract
The work done under Contract No. DA-18-108-CML6678 and the extension of this contract can best be reported in three categories. The first, Part A, is a continuation of work done on prior grants and contracts to complete the series of compounds which can be described as alpha-3nitrophenoxy-omega-(3-nitro-5-dimenthylcarbamyloxyphenoxy)-alkanes and alpha-(3-nitrophenoxy)omega-(3-nitro-5-hydroxyphenoxy)-alkanes. Some 1,10-bis(3-nitro-5-dimethylcarbamyloxyphenoxy)decane was also prepared. Part B of this report contains the methods used for the preparation of various intermediates to be used in the synthesis of 1,3-bid(5-dimethylcarbamyloxy-3pyridoxy)-propane and 1-(3-pyridoxy)-3-(5dimethylcarbamyloxy-3-pyridoxy)-propane. Part C contains the methods of preparing various aliphatic compounds containing two tertiary amine groups and two alcohol groups, or groups which could be converted to alcohols. Much of this work was left in an incomplete state when it was decided to abandon work with the aliphatic compounds. (Author)
Document Details
- Document Type
- Technical Report
- Publication Date
- Mar 31, 1964
- Accession Number
- AD0439242
Entities
People
- Harry L. Hennessy
- J. Philip Mason
- John E. Eaton
- Pierre D. Lord
- Raymond G. Mcinnis
Organizations
- Boston University