FAR INFRARED SPECTRA OF CRYSTALLINE ACETYLENES, C2H2 AND C2D2.

Abstract

The far infrared spectra of polycrystalline films of acetylene and fully deuterated acetylene were recorded at 77 k, using a commercial Michelson Interferometer. Two sharp bands are observed for each crystal, and the frequency change on deuteration leads to their assignment as translational lattice modes. From these and other spectroscopic results, deductions concerning the crystal structure, which has not been directly measured at this temperature, are made, and it is concluded that the most likely factor group is of D2h symmetry with two molecules per unit cell on C2h sites, a structure similar to those of crystalline carbon disulfide and the halogens. It is shown that the two-fold axis at the site does not coincide with the molecular axis, as previously implied. (Author)

Document Details

Document Type
Technical Report
Publication Date
Nov 01, 1965
Accession Number
AD0474545

Entities

People

  • Andrea Anderson
  • William Hayden Smith

Organizations

  • Princeton University

Tags

DTIC Thesaurus Topics

  • Acetylenes
  • Alkynes
  • Crystal Structure
  • Crystals
  • Electromagnetic Spectra
  • Infrared Spectra
  • Inorganic Carbon Compounds
  • Interferometers
  • Michelson Interferometers
  • Polycrystals
  • Spectra

Readers

  • Materials Science and Engineering.
  • Molecular Photonics/Laser Physics
  • Organic Chemistry