Thermal Decomposition Studies of a New Perchlorate Oxidizer

Abstract

The initial step in the thermal decomposition of methylenedioxyamine diperchlorate occurs at 60 C with the loss of a perchloric acid group to form the monoacid salt as an intermediate. As the temperature increases, the latter undergoes a concerted cyclization - cleavage reaction to form formamide and hydroxylammonium perchlorate. Mass spectrometry was used to formulate a working hypothesis for the decomposition. The existence of each of the postulated intermediates in the reaction was verified by independent experiments.

Open PDF

Document Details

Document Type
Technical Report
Publication Date
May 01, 1969
Accession Number
AD0503916

Entities

People

  • Berge B. Goshgarian
  • Francisco Q. Roberto
  • Raymond E. Foscante

Organizations

  • Air Force Research Laboratory

Tags

Communities of Interest

  • Weapons Technologies

DTIC Thesaurus Topics

  • Air Force
  • Body Weight
  • Chemical Products
  • Chemical Reactions
  • Crystal Structure
  • Insensitive Explosives
  • Mass Spectra
  • Mass Spectrometers
  • Mass Spectrometry
  • Materials
  • Measurement
  • Perchloric Acid
  • Phase
  • Pressure Measurement
  • Propellants
  • Spectra
  • Spectrometry

Fields of Study

  • Chemistry

Readers

  • Analytical Chemistry
  • Organic Chemistry
  • Rocket Propulsion.