THE CONTROLLED THERMAL DECOMPOSITION OF CELLULOSE NITRATE. VII. CARBONYL COMPOUNDS.

Abstract

An investigation of the carbonyl compounds formed from the ignition of cellulose nitrate was made. Isolated as the 2,4-dinitrophenylhydrazine derivatives were acetone, acetaldehyde, formaldehyde, methylglyoxal, glyoxal, mesoxaldehyde and hydroxypyruvaldehyde. A gas chromatographic study of the cellulose nitrate (cast from ethyl acetate) ignition products demonstrated the presence therein of acetaldehyde, acetone, acrolein, ethyl acetate, hydrogen cyanide and a now, unidentified substance which is not a carbonyl compound. Ethanol is not a product of ignition of cellulose nitrate. The origin of the compoundss isolated is discussed. (Author)

Document Details

Document Type
Technical Report
Publication Date
Oct 28, 1959
Accession Number
AD0606348

Entities

People

  • G. P. Arsenault
  • M. L. Wolfrom

Organizations

  • Ohio State University

Tags

DTIC Thesaurus Topics

  • Acetaldehyde
  • Acroleins
  • Aldehydes
  • Cellulose
  • Chemical Compounds
  • Chemical Reactions
  • Cyanides
  • Decomposition
  • Dissociation
  • Formaldehyde
  • Hydrogen
  • Hydrogen Cyanide
  • Ignition
  • Lysis
  • Nitrocellulose

Readers

  • Analytical Chemistry
  • Organic Chemistry