CHEMILUMINESCENT SYSTEMS

Abstract

The survey of chemiluminescent autoxidation reactions has been continued. Of the forty odd additional compounds screened, the large majority show enhanced chemiluminescence over background in potassium t-butoxide dissolved in dimethylsulfoxide (DMSO). About one-third of the reactants exceeded 1% of the standard source brightness. The latter group includes several substituted benzoins, demonstrating the generality of the chemiluminescence of the oxidation of this class of stable radicals. The chemiluminescence of indole and several 3-substituted indoles has been investigated. In t-Bu OK and DMSO solution, 0.005 M skatole is about fifty times brighter than the standard source. At a base concentration of 0.067 M the brightness is an increasing function of skatole concentration to almost 0.1 mole/liter. At this concentration the brightness is 400 times that of the standard, or about half that of 0.005 M luminol. Emission and fluorescence spectra (uncorrected) have been obtained for the basic skatole solution and for the addition, 0.0001 M fluorescein.

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Document Details

Document Type
Technical Report
Publication Date
Mar 22, 1965
Accession Number
AD0613013

Entities

People

  • Abraham W. Berger

Organizations

  • Monsanto

Tags

Communities of Interest

  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Alkenes
  • Brightness
  • Chemiluminescence
  • Corporations
  • Cyclic Hydrocarbons
  • Efficiency
  • Emission
  • Emission Spectra
  • Fluorescence
  • Free Radicals
  • Hydrazines
  • Instrumentation
  • Laser Dyes
  • Luminescence
  • Quantum Efficiency
  • Spectra
  • Standards

Fields of Study

  • Chemistry

Readers

  • Chemistry (specifically Chemical Fluorescence)
  • Organic Chemistry
  • Systems Analysis and Design