HETEROCYCLIC ORGANOBORON COMPOUNDS. PART III. SYNTHESIS OF PHENYLBORACYCLOPENTANE AND THE INFRARED SPECTRA OF THIS AND OTHER PHENYLBORON COMPOUNDS,

Abstract

An improved synthesis of phenylboracyclopentane by the reaction of phenylborane-triethylamine with butadiene is reported, but the preparation of this compound from phenylboron difluoride and 1,4-dilithiobutane could not be confirmed. The infrared spectrum of phenylboracyclopentane is analysed in detail and shown to be consistent with the proposed structure. The spectra of phenylboron difluoride and phenylborane-triethylamine are also recorded and assignments made. (Author)

Document Details

Document Type
Technical Report
Publication Date
Apr 15, 1964
Accession Number
AD0615692

Entities

People

  • John Wright
  • N. N. Greenwood

Organizations

  • Newcastle University

Tags

DTIC Thesaurus Topics

  • Butadienes
  • Diffraction
  • Electromagnetic Spectra
  • Infrared Spectra
  • Spectra
  • Ultraviolet Spectra
  • Wave Phenomena

Fields of Study

  • Chemistry

Readers

  • Combustion science or combustion engineering.
  • Geochemistry
  • Materials Science and Engineering.