USE OF REACTIVE ATMOSPHERES FOR THE TREATMENT OF B. C. C. METALS.

Abstract

The sintering of tungsten compacts impregnated with solutions of palladium chloride or nickel chloride was studied. The results of bend tests indicated no ductility in the activation-sintered tungsten specimens. Postsintering treatments for improving the ductility of palladium- and nickel-activation sintered specimens were found to be effective. The sintering kinetics of tungsten activated by nickel and palladium are being studied. The optimum concentration of the activator was found to be 0.130 wt.% of nickel and 0.317 wt.% of palladium. Additions of thoria, to stabilise the tungsten grain, have no effect on this. Rate exponents and activation energies for the sintering process were determined, and a model for theoretical purposes was devised. Test-pieces were prepared under standardised conditions (with optimum concentrations of activators) for studies of the de-embrittling treatments. (Extracted)

Document Details

Document Type
Technical Report
Publication Date
Mar 31, 1965
Accession Number
AD0616273

Entities

People

  • I. J. Toth

Organizations

  • University of Surrey

Tags

Communities of Interest

  • Materials and Manufacturing Processes

DTIC Thesaurus Topics

  • Atmospheres
  • Chlorides
  • Ductility
  • Energy
  • Heat Of Activation
  • Kinetics
  • Metals
  • Palladium
  • Sintering
  • Tungsten

Fields of Study

  • Materials science

Readers

  • Powder metallurgy of Titanium alloys.
  • Surface Engineering/Surface Coating Technology.