X-RAY POWDER PATTERNS FOR THE IDENTIFICATION OF SOME N-ALKANONE SEMICARBAZONES.

Abstract

The interplanar spacings obtained from the X-ray powder patterns of a series of structurally related semicarbazones were used to unequivocally identify the ketones from which the derivatives were prepared. The advantages of the proposed over the currently used melting points to identify the compounds were cited. The method was found to be applicable to slightly contaminated mixtures of semicarbazones. (Author)

Document Details

Document Type
Technical Report
Publication Date
Dec 16, 1964
Accession Number
AD0618959

Entities

People

  • Bruce W. Brodman
  • Jack Radell
  • Kimball Kramer

Tags

DTIC Thesaurus Topics

  • Chemical Compounds
  • Chemical Synthesis
  • Chemistry
  • Identification
  • Isothermal Processes
  • Melting
  • Melting Point
  • Organic Chemistry
  • Phase Transformations
  • Semicarbazides
  • X Rays

Readers

  • Analytical Chemistry
  • Materials Science and Engineering.

Technology Areas

  • Space