DETERMINATION OF NICKEL IN PHOSPHATIZING BATHS BY THE X-RAY SPECTROGRAPHIC TECHNIQUE.

Abstract

The purpose of the work was to develop a fast accurate method for the determination of nickel in phosphating baths. To accomplish this, basic nickel carbonate is known amounts was added to aliquots of phosphating solution. To prevent precipitation of solids during analysis, hydrochloric acid was added to the aliquots. A number of samples, taken from several different phosphating baths and stabilized in the manner described above, were subjected to X-ray spectrographic analysis for nickel. The results obtained from these analyses showed that the method described is a fast accurate method for the determination of nickel in phosphate baths. (Author)

Document Details

Document Type
Technical Report
Publication Date
Jun 01, 1965
Accession Number
AD0620141

Entities

People

  • W. D. Mchenry
  • W. O. Crawford

Tags

DTIC Thesaurus Topics

  • Acids
  • Carbonates
  • Chemical Compounds
  • Hydrochloric Acid
  • Precipitation
  • X Rays

Readers

  • Approximation Theory.
  • Surface Engineering/Surface Coating Technology.