The Radiation Chemistry of Acetylenic Compounds

Abstract

G-values for radiolysis products were determined for propyne and butyne-1 in the vapor phase and for butyne-1, butyne-2, pentyne-1, pentyne-2, hexyne-3, acetonitrile and propionitrile in the liquid phase. The rupture of a C-H bond probably from a carbon beta to the triple bond results in H2, coupling products, and H atom addition. H atom addition leads to mono and poly olefins. The rupture of a C-C bond results in fragmentation in the vapor phase but recombination to form 1.2-diolefins in liquid phase. Both alpha and beta C-C bond rupture occur. Alkyl benzene-alkyne trimers-form, probably by excitation. Analogous C3N3 ring compounds may form but were not detected. Gas chromatography techniques for alkyne and nitrile analyses are described.

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Document Details

Document Type
Technical Report
Publication Date
Jul 01, 1965
Accession Number
AD0621719

Entities

People

  • Herbert H. Barber
  • Larry A. Harrah
  • Roger E. Rondeau
  • Thomas D. Nevitt

Tags

Communities of Interest

  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Air Force
  • Air Force Facilities
  • Alkenes
  • Alkynes
  • Chemical Synthesis
  • Chemistry
  • Detectors
  • Gamma Rays
  • Gas Chromatography
  • Mass Spectrometry
  • Materials
  • Materials Laboratories
  • Measurement
  • Organic Chemistry
  • Radiation Chemistry
  • Silver Compounds
  • Spectrometry

Fields of Study

  • Chemistry

Readers

  • Materials Science and Engineering.
  • Organic Chemistry
  • Petroleum Engineering