A FLUOROMETRIC PROCEDURE FOR MEASURING THE ACTIVITY OF DEHYDROGENASES.

Abstract

A simple, direct, fluorometric method is described for measuring the activity of dehydrogenases. The method is based upon the conversion of the nonfluorescent material resazurin to the highly fluorescent compound resorufin, in conjunction with the nicotinamide adenine dinucleotide-reduced nicotinamide adenine dinucleotide (NAD(+)-NADH) system. By the procedures described, approximately 0.00010 to 0.1000 unit/ml of lactic acid dehydrogenase, alcohol dehydrogenase, malic acid dehydrogenase, glutamic acid dehydrogenase, glucose6-phosphate dehydrogenase, L-alphs-glycero phosphate dehydrogenase (GPDH), and glycerol dehydrogenase (GDH) may be determined with standard deviations of approximately =1.0%. Similarly, diaphorase, 0.000400 to 0.0800 unit/ml, resazurin, 0.00000001 to 0.00001 M, and NADH, 0.0000002 to 0.00002 M, may be determined with standard deviations of =0.5%, =0.8%, and =0.5%, respectively. (Author)

Document Details

Document Type
Technical Report
Publication Date
Aug 01, 1965
Accession Number
AD0622341

Entities

People

  • David N. Kramer
  • George G. Guilbault

Organizations

  • Edgewood Chemical Biological Center

Tags

DTIC Thesaurus Topics

  • Alcohols
  • Biomolecules
  • Carboxylic Acids
  • Chemical Compounds
  • Conversion
  • Data Science
  • Glutamic Acid
  • Glycerols
  • Lactic Acid
  • Malic Acid
  • Materials
  • Organic Compounds
  • Standards
  • Sugar Alcohols

Readers

  • Analytical Chemistry
  • Molecular and Cellular Biochemistry