LIGHT ATTENUATION BY PHOTOCHEMICAL MEANS: PHOTOCHROMISM

Abstract

It was found that the photochromism of 2-(2,4-dinitrobenzyl)pyridine is not limited to this compound, but is the common property of a class of aromatic nitro compounds which possesses certain structural characteristics: the presence of a nitro and a methenyl group ortho to each other. Solvents were found to have a marked effect on the rate of the fading reactions; As were substituents in the para position of the aromatic ring of o-nitrobenzylpyridines. It was found that on irradiation with ultraviolet light, 3,3'-dinitro-4,4'-di(2-pyridylmethyl)azoxybenzene undergoes simultaneously aci-nitro tautomerization and geometrical isomerization. A new class of photochromic nitro compounds was discovered. The essential structural requirement for photochromism in these 1-aryl-2-nitroalkenes is that the nitro and phenyl groups bear a cis relationship with respect to each other. It was shown that some of the simpler o-nitrobenzyl compounds, such as o-nitroluene, are not only photochromic, but give relatively stable free radicals when irradiated with ultraviolet light. These radicals were identified as phenyl nitroxides.

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Document Details

Document Type
Technical Report
Publication Date
Jun 01, 1966
Accession Number
AD0634651

Entities

People

  • Aaron L. Bluhm
  • E. T. Strom
  • Julius Weinstein
  • Margaret E. Langmuir

Organizations

  • United States Army Soldier Systems Center

Tags

Communities of Interest

  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Absorption
  • Chemical Reaction Properties
  • Electron Spin Resonance
  • Free Radicals
  • Ground State
  • Heat Of Activation
  • Line Spectra
  • Low Temperature
  • Measurement
  • Nitro Compounds
  • Photolysis
  • Radiation
  • Spectra
  • Spin Resonance
  • Thermodynamic Properties
  • Ultraviolet Spectra
  • Visible Spectra

Fields of Study

  • Chemistry

Readers

  • Chemistry (specifically Chemical Fluorescence)
  • Organic Chemistry