THE OSCILLATOR STRENGTH OF LEAD (II) ION IN POTASSIUM CHLORIDE SINGLE CRYSTALS.

Abstract

KCl single crystals, homogeneously doped with PbCl2, were analyzed for lead by the dithizone method, and the optical absorbance at 273 millimicrons was determined. The absorbance at 273 millimicrons in samples of a given lead concentration depended on original purity of the KCl, the atmosphere under which the crystal was grown, and the thermal treatment prior to measurement. The oscillator strength was found to be 0.11 plus or minus 0.02 in crystals of highest purity, grown under dry HCl or argon, and rapidly quenched from 600C. This agrees with the value reported by Sibley, Sonder, and Butler. When reagent grade KCl was used, or the atmosphere was air, the average oscillator strength found was 0.086, which is close to the value reported by Kaifu. (Author)

Document Details

Document Type
Technical Report
Publication Date
Aug 25, 1966
Accession Number
AD0640171

Entities

People

  • Allen B. Scott
  • Robert E. Holmes

Organizations

  • Oregon State University

Tags

DTIC Thesaurus Topics

  • Atmospheres
  • Azo Compounds
  • Chemical Compounds
  • Chlorides
  • Crystals
  • Measurement
  • Oscillators
  • Potassium
  • Potassium Chloride
  • Single Crystals

Readers

  • Electrochemical Engineering/ Fuel Cell Technologies
  • Materials Science and Engineering.