AN INVESTIGATION OF THE RHEOLOGY OF GELS,

Abstract

The report describes work accomplished on the rising sphere rheometer and efforts to develop a standard gel to be used for interlaboratory comparisons both on the rising sphere and on the Brookfield viscometer. The construction details and wiring for the rheometer and an optical method for checking the rate of rise are presented. It was found that the accuracy of the rheometer could be greatly improved by expanding and displaying the output scale on a Leeds and Northrup recorder. Several batches of a 'standard' gel (0.15-percent Carbopol 940 in water) were tried but gave inconsistent results with this rheometer, as well as not giving consistent densities. The results of these tests seem to indicate that Carbopol 940 is not suitable as a component in standard gels, if unsophisticated mixing methods are to be used. In addition, Cabosil (2 concentrations tried), Methocell 90HG-D65 (3 concentrations tried), and Cellosize 5229-JJ were tried with water all mixed by hand shaking. All samples failed to demonstrate reasonable yield values or settled on standing. (Author)

Document Details

Document Type
Technical Report
Publication Date
Aug 22, 1966
Accession Number
AD0641484

Entities

People

  • Barry D. Allan
  • Joel H. Blatt

Organizations

  • United States Army Aviation and Missile Command

Tags

DTIC Thesaurus Topics

  • Accuracy
  • Construction
  • Instrumentation
  • Measuring Instruments
  • Recording Systems
  • Rheology
  • Rheometers
  • Standards
  • Viscometers

Readers

  • Fluid Dynamics.
  • Mathematics or Statistics
  • Polymer Science and Engineering.