A Study of the Zirconia-Hafnia System

Abstract

A definitive study of phase relationships in the ZrO2-HfO2 system was conducted. Metallographic, X-ray, differential-thermal, and microprobe analyses were applied to annealed and quenched specimens of arc-melted compositions. The system forms a continuous series of solid solutions in the low-temperature monoclinic structure as well as the high-temperature tetragonal structure. There is a relatively small intervening monoclinic plus tetragonal two-phase solid solution field. This field lies approximately on a straight line connecting the inversion temperatures of the two oxides. The melting points of ZrO2-HfO2 compositions likewise lie roughly on a line connecting the melting point of each oxide. There are no intervening complex oxides. Effort was also directed toward a better definition of the high-temperature, high-hafnium region of the Hf-O system. This study was brought to a conclusion and a final Hf-O diagram is presented.

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Document Details

Document Type
Technical Report
Publication Date
Apr 01, 1964
Accession Number
AD0658041

Entities

People

  • R. F. Domagala

Organizations

  • IIT Research Institute

Tags

Communities of Interest

  • Advanced Electronics
  • Space

DTIC Thesaurus Topics

  • Air Force
  • Air Force Facilities
  • Arc Melting
  • Controlled Atmospheres
  • Differential Thermal Analysis
  • Heat Energy
  • Heaters
  • High Temperature
  • Low Temperature
  • Materials
  • Melting
  • Melting Point
  • Metal Oxides
  • Metals
  • Oxides
  • Solid Solutions
  • X Rays

Readers

  • Calculus or Mathematical Analysis
  • Materials Science and Engineering.
  • Systems Analysis and Design